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Robust Synthesis of F-BODIPYs

dc.contributor.authorBeh, Michael
dc.contributor.authorDouglas, Katherine
dc.contributor.authorHouse, Kelsey
dc.contributor.authorMurphy, Alexandra
dc.contributor.authorSinclair, Jackson
dc.contributor.authorThompson, Alison
dc.date.accessioned2017-08-22T14:36:15Z
dc.date.available2017-08-22T14:36:15Z
dc.date.issued2016
dc.description.abstractF-BODIPYs are widely used in applications that rely upon their highly tunable optical properties. A protocol is established for the high-yielding synthesis of F-BODIPYs involving non-anhydrous reagents and not requiring precautions to exclude moisture. This simple and robust strategy simply requires a second addition of NEt3 and BF3 OEt2, midway through the reaction period. The ratio and amounts of NEt3 and BF3 OEt2 used in each aliquot are critical to success. The protocol can be completed using bench-dry apparatus, without need to achieve and maintain anhydrous conditions or solvents.
dc.identifier.citationPublisher's version: Beh, Michael; Douglas, Katherine; House, Kelsey; Murphy, Alexandra; Sinclair, Jackson; and Thompson, Alison. Robust Synthesis of F-BODIPYs. Org. Biomol. Chem. 2016, 14, 11473-11479. DOI: 10.1039/c6ob02238cen_US
dc.identifier.urihttp://hdl.handle.net/10222/73139
dc.language.isoenen_US
dc.publisherRoyal Society of Chemistryen_US
dc.relation.ispartofOrganic and Biomolecular Chemistryen_US
dc.titleRobust Synthesis of F-BODIPYsen_US
dc.title.alternativeOrg. Biomol. Chem.en_US
dc.typeArticleen_US

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